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Perfumes and their preparation

Chapter 573: Eau de Botot.
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About This Book

The work surveys the development and principles of perfumery, reviews aromatic substances from plant and animal sources and their chemical counterparts, and explains methods for extracting, testing, and identifying adulteration. It presents classifications of perfumes and detailed recipes for handkerchief waters, dry sachets, fumigants, and ammoniacal or acid scents, followed by practical instructions for producing essences and extracts. Later sections cover hygienic and cosmetic perfumery with formulas for skin, hair, and mouth preparations, hair dyes and depilatories, colorants, and manufacturing utensils, offering guidance on material selection and wholesale production.

Tonka beans 1 lb.
Lard 8 lb.

The powdered beans are stirred into the melted fat, in which they remain for several days, the fat being agitated from time to time; when it smells strong enough, it is strained through fine linen, and the tonka beans are treated with another quantity of fat.

Violet Pomade (Pomade des Violettes).

Lard 4 lb.
Cassie pomade 3 lb.
Rose pomade 2 lb.
Violet pomade 2 lb.

Vanilla Cream (Crême de Vanille).

Vanilla 7 oz.
Lard 6 lb.

In making this pomade the material is treated the same as in preparing tonka pomade. Ordinary vanilla pomade is made by triturating:

Peru balsam 7 oz.
Lard 2 lb.
Expressed oil of almond 2 lb.

First triturate the balsam with the almond oil and gradually add the lard. Another, much better process is the following:

Vanilla Pomade.

Vanillin 80 grains.
Peru balsam ½ oz.
Lard 6 lb.

Dissolve the vanillin and balsam of Peru in about 4 oz. of alcohol. Melt the lard at as low a temperature as possible, then add the solution, stir until it is well incorporated, and afterward repeatedly until the mass is cold.

Pomade Philocome.

Huile antique of cassie 1 lb.
Huile antique of jasmine 1 lb.
Huile antique of orange flower 3½ oz.
Huile antique of rose 3½ oz.
Huile antique of tuberose 3½ oz.
Huile antique of violet 1 lb.
Paraffin 10½ oz.
Wax 14 oz.

This pomade has a delightful odor but is expensive; an inferior and much cheaper philocome is made as follows:

Expressed oil of almond 8 lb.
Paraffin ½ lb.
Wax 14 oz.
Oil of bergamot 4¼ oz.
Oil of lemon 1¾ oz.
Oil of lavender ¾ oz.
Nutmeg 75 grains.
Cloves 75 grains.
Cinnamon 75 grains.

Pomades are usually colored—rose pomade, red; reseda pomade, green; violet pomade, violet, etc. For this purpose aniline colors are frequently used; they must be dissolved in glycerin and added to the fat, as they are insoluble in the latter. The coloring matter is added when the pomades are finished, before they are allowed to congeal.

B. Hair Oils.

These differ from pomades mainly by containing huiles antiques instead of washed pomades; they are therefore more or less liquid and are used for the hair as much as pomades.

Benzoated Oil (Huile à Benjamin).

Sublimed benzoic acid 5 oz.
Expressed oil of almond 4 lb.

The acid must be dissolved in the hot oil.

Huile à l’Ess-Bouquet.

Oil of rose 150 grains.
Oil of reseda 3½ oz.
Oil of violet 150 grains.
Tincture of musk 75 grains.
Almond oil 6 lb.

The essential oils are mixed, and the almond oil is added in small portions under continual stirring.

Heliotrope Hair Oil (Huile Héliotrope).

Huile antique of jasmine 10½ oz.
Huile antique of rose 2 lb.
Huile antique of orange flower 5½ oz.
Huile antique of tuberose 5½ oz.
Huile antique of vanilla 1 lb.
Oil of bitter almond 150 grains.
Oil of clove 75 grains.

Jasmine Hair Oil (Huile de Jasmin).

Expressed oil of almond 4 lb.
Huile antique of jasmine. 7 oz.
Oil of bergamot 1 oz.
Oil of lemon 150 grains.

Oil of Swiss Herbs.

Expressed oil of almond 4 lb.
Oil of bergamot 150 grains.
Oil of lemon 75 grains.
Oil of lavender 75 grains.
Oil of peppermint 150 grains.
Oil of cinnamon 75 grains.

Oil of Burdock Root.

Expressed oil of almond 4 lb.
Burdock root 1 lb.
Oil of bergamot 1 oz.
Oil of lemon 1 oz.
Oil of rose ¾ oz.

The burdock root is macerated for two days in the warm oil, which is then filtered and the other ingredients are added.

Macassar Oil.

Expressed oil of almond 4 lb.
Alkanet root 7 oz.
Oil of clove 75 grains.
Oil of mace 75 grains.
Oil of rose 75 grains.
Oil of cinnamon ½ oz.
Tincture of musk 75 grains.

The alkanet root in coarse powder must be macerated in the warm almond oil until it acquires a deep red color.

Peru Hair Oil.

Peru balsam 3½ oz.
Storax 1¾ oz.
Expressed oil of almond 8 lb.

Mix by stirring, and allow to settle for two weeks in a completely filled bottle.

Huile Philocome.

Expressed oil of almond 4 lb.
Huile antique of cassie 1 lb.
Huile antique of jasmine 28 oz.
Wax 3½ oz.
Spermaceti 1¾ oz.
Oil of neroli 1 oz.
Oil of rose 150 grains.
Oil of cinnamon 75 grains.

Portugal Oil.

Expressed oil of almond 4 lb.
Oil of bergamot 1 oz.
Oil of lemon 150 grains.
Oil of neroli 75 grains.
Oil of orange flower 75 grains.
Oil of orange peel ¾ oz.
Oil of cinnamon 75 grains.

Tonka Oil.

Tonka beans 1 lb.
Expressed oil of almond 4 lb.

Inclose the powdered tonka beans in a linen bag, which is hung into the cold oil and allowed to macerate for several weeks. The same process is employed for the following:


Vanilla Oil.

Vanilla 7 oz.
Almond oil 4 lb.

Or,

Vanillin 80 grains.
Expressed oil of almond 4 lb.

CHAPTER XXIV.
PREPARATIONS FOR THE CARE OF THE MOUTH.

Besides the red lips and the gums, the teeth in particular ornament the mouth. Unfortunately there are but few persons who can boast of a perfectly healthy set of teeth, which is found as a normal condition only among savages and animals. The chief causes of the admitted fact that most persons have some defect in the mouth—bad teeth, pale gums, offensive odor—lie in part in our civilization with the ingestion of hot and sometimes sour food, in part in the lack of attention bestowed on the care of the mouth by many people. The care of the mouth is most important after meals and in the morning; particles of food lodge even between the most perfect teeth and undergo rapid decomposition in the high temperature prevailing in the mouth. This gives rise to a most disagreeable odor, and the decomposition quickly extends to the teeth.

Perfectly normal healthy teeth consist of a hard, brilliant external coat, the enamel, which opposes great resistance to acid and decomposing substances. But unfortunately the enamel is very sensitive to changes of temperature and easily cracks, thus admitting to the bony part of the teeth such deleterious substances and leading to their destruction. The bulk of the tooth consists of a porous mass of bone which is easily destroyed, and thus the entire set may be lost.

Hygienic perfumery is able to offer to the public means by which a healthy set of teeth can be kept in good condition and the disease arrested in affected teeth, and by which an agreeable freshness is imparted to the gums and lips. While true perfumes may be looked upon as more or less of a luxury, the hygiene of the mouth is a necessity; for we have to deal with the health and preservation of the important masticatory apparatus which is necessary to the welfare of the whole body, so that the æsthetic factor occupies a secondary position, or rather results as a necessary consequence from a proper care of the mouth.

With no other hygienic article have so many sins been committed as with those intended for the teeth; we have had occasion to examine a number of tooth powders, some of them very high-priced, which were decidedly injurious. Thus we have known of cases in which powdered pumice stone, colored and perfumed, has been sold as a tooth powder. Pumice stone, however, resembles glass in its composition and acts on the teeth like a fine file which rapidly wears away the enamel and exposes the frail bony substance. It needs no further explanation to prove the destructive effects of such a powder on the teeth.

Many person prize finely powdered wood charcoal as a tooth powder, and to some extent they are right. Wood charcoal always contains alkalies which neutralize the injurious acids, besides traces of products of dry distillation which prevent decomposition. But these valuable properties are counteracted by the fact that charcoal is always more or less gritty, or, being insoluble, will lodge between the teeth and form the nucleus for the lodgement of other substances.

In compounding articles for the mouth and teeth—tooth powders and mouth washes—the objects aimed at are to neutralize the chemical processes that injure the teeth and gums, and to restore freshness and resisting power to the relaxed gums and mucous membranes.

Remnants of food left in the mouth after meals soon develop acids which attack the teeth; they are neutralized by basic substances or alkalies which counteract them.

The formation of organic acids from food remnants is caused by microscopic fungi (schizomycetes) which adhere to the teeth (so-called tartar) in the absence of cleanliness; against these parasites there are at our disposal a number of substances which kill them rapidly and thus for a time arrest the process of decomposition; they are therefore called antiseptics.

Another group of ingredients acts especially on such abnormal conditions of the membranous and fleshy parts of the mouth as manifest themselves by colorless, easily bleeding gums. It is mainly compounds of the tannin group which strengthen the gums and are known as astringents.

In compounding articles for the teeth it has thus far unfortunately not been customary to combine several of the substances having the above properties, the general rule being to incorporate only one in the composition, and some so-called tooth lotions consist even of aromatics alone. Such articles perfume the mouth, but have no hygienic effect upon it.

Among the essential oils, however, there is one which should form a part of every article intended for the care of the mouth, provided it can remain unchanged in the presence of the other ingredients, which would not be the case where permanganate of potassium is used. Oil of peppermint and other mint oils exert a very refreshing influence on the mucous membranes of the mouth, in which they leave a sensation of freshness lasting for some time.

We give below a number of formulas for the manufacture of articles for the care of the mouth, as to the value of which the reader can form his own opinion from what has been stated. Finally it may be observed that several of the so-called secret preparations for the care of the mouth are arrant humbugs, worthless substances being sold at exorbitant prices and, worse yet, lacking the vaunted hygienic effect owing to their chemical composition.

The articles for the care of the mouth and teeth may be divided into tooth pastes, tooth powders, tooth tinctures or lotions, and mouth washes.

A. Tooth Pastes.

Tooth Soap (Savon Dentifrice).

Soap 2 lb.
Talcum 2 lb.
Orris root 2 lb.
Sugar 1 lb.
Water 1 lb.
Oil of clove 150 grains.
Oil of peppermint ¾ oz.

The soap should be good, well-boiled tallow soap; it is mixed with the other ingredients (the sugar is to be previously dissolved in the water) by thorough and prolonged stirring, and is usually sold in shallow porcelain boxes. The talcum or French chalk is a soft mineral with a fatty feel and is a common commercial article.

This tooth soap and other similar preparations for the care of the mouth are frequently colored rose red. Of course only harmless colors can be used. The most appropriate are rose madder lake and carmine.

Tooth Paste (Pâte Dentifrice).

Prepared chalk 2 lb.
Orris root 2 lb.
Sugar 2 lb.
Water 1 lb.
Madder lake ¾ to 1½ oz.
Oil of lavender 150 grains.
Oil of mace 150 grains.
Oil of clove 150 grains.
Oil of peppermint 1 oz.
Oil of rose 150 grains.

The prepared chalk used in this and many other articles is pure precipitated carbonate of lime. It is made from pieces of white marble, the offal from sculptors’ workshops, which are placed in wide porcelain or glass vessels and covered with hydrochloric acid, when abundant vapors of carbonic acid are given off. When the development of carbonic acid has ceased, the liquid is allowed to stand at rest for several days with an excess of marble, whereby all the iron oxide is separated. This is necessary, otherwise the preparation would not be white, but yellowish. The liquid is filtered and treated with a solution of carbonate of soda (sal soda), in water as long as any white precipitate results. This precipitate is washed with pure water on a filter, and when slowly dried it forms a fine, brilliant white powder. Crystalline calcium chloride may also be purchased, dissolved in water, and treated with the soda solution to obtain the white precipitate. The quantity of madder lake in the above formula is given within the limits to form light or dark red tooth paste.

B. Tooth Powders.

Quinine Tooth Powder.

Prepared chalk 2 lb.
Starch flour 1 lb.
Orris root, powdered 1 lb.
Sulphate of quinine ¾ oz.
Oil of peppermint 150 grains.

Cinchona Bark Tooth Powder.

Cinchona bark, powdered 1 lb.
Prepared chalk 2 lb.
Myrrh, powdered 1 lb.
Orris root, powdered 2 lb.
Cinnamon, powdered 1 lb.
Carbonate of ammonia 2 lb.
Oil of clove ¾ oz.

Borated Tooth Powder.

Borax, powered 1 lb.
Prepared chalk 2 lb.
Myrrh, powdered ½ lb.
Orris root, powdered ½ lb.
Cinnamon, powdered ½ lb.

Homœopathic Chalk Tooth Powder.

Prepared chalk 4 lb.
Starch flour 5½ oz.
Orris root, powdered ½ lb.
Oil of cinnamon 1 oz.

Camphorated Chalk Tooth Powder.

Prepared chalk 4 lb.
Camphor 1 lb.
Orris root, powdered 2 lb.
Cinnamon, powdered ½ lb.

Charcoal Tooth Powder.

Charcoal, powdered 4 lb.
Cinchona bark, powered 1 lb.
Oil of bergamot ½ oz.
Oil of lemon 1 oz.

The charcoal must be derived from some soft wood; willow, poplar, or buckthorn are among the most appropriate.

Cuttlefish-Bone Tooth Powder.

Prepared chalk 4 lb.
Cuttlefish-bone, powdered 2 lb.
Orris root, powdered 2 lb.
Oil of bergamot ¾ oz.
Oil of lemon 1½ oz.
Oil of neroli 150 grains.
Oil of orange ¾ oz.

Cachous Aromatisées.

Cachous are of a pillular composition, and used not so much for the teeth as to impart fragrance to the breath.

They are made as follows:

Gum acacia 1½ oz.
Catechu, powdered 2¾ oz.
Licorice juice 1¼ lb.
Cascarilla, powdered ¾ oz.
Mastic, powdered ¾ oz.
Orris root, powdered ¾ oz.
Oil of clove 75 grains.
Oil of peppermint ½ oz.
Tincture of ambergris 75 grains.
Tincture of musk. 75 grains.

Boil the solids with water until a pasty mass results which becomes firm on cooling. The aromatics are then added, and the mass is rolled into pills which are covered with genuine silver foil. One of these pills suffices to remove the odor of tobacco, etc., completely from the mouth.

Pastilles Orientales.

Sugar 8 lb.
Carmine 75 grains.
Gum acacia 2 lb.
Musk 15 grains.
Oil of rose 75 grains.
Oil of vetiver 15 grains.
Civet 15 grains.
Tartaric acid 150 grains.

Add the essential oils to the powdered solids, mix intimately, and add enough water to form a stiff dough, to be made into pills which when chewed remove the odor of tobacco or other unpleasant odors.

Rose Tooth Powder.

Prepared chalk 4 lb.
Orris root, powdered 2 lb.
Madder lake 1¾ to 2½ oz.
Oil of rose ½ oz.
Oil of santal 150 grains.

Sugar Tooth Powder.

Bone-ash 4 lb.
Orris root, powdered 4 lb.
Sugar, powdered 2 lb.
Oil of bergamot ¾ oz.
Oil of citron ½ oz.
Oil of mace 75 grains.
Oil of neroli 75 grains.
Oil of orange 150 grains.
Oil of rosemary ¾ oz.

Chinese Tooth Powder.

Pumice stone 4 lb.
Starch flour. 1 lb.
Madder lake 1¾ oz.
Oil of peppermint ¾ oz.

The pumice stone must be ground into the finest powder and levigated, before being mixed with the other ingredients. Note our remarks on pumice stone on page 258.

C. Tooth Tinctures (Lotions) and Mouth Washes (Essences Dentifrices).

Eau Anathérine.

Guaiac wood 3½ oz.
Myrrh 8 oz.
Cloves 5½ oz.
Santal wood 5½ oz.
Cinnamon 1¾ oz.
Alcohol 4 qts.
Rose water 2 qts.
Oil of mace. 75 grains.
Oil of rose 75 grains.
Oil of cinnamon 75 grains.

The solids are macerated in the alcohol, the essential oils are dissolved in the filtered liquid, and lastly the rose water is added.

Eau de Botot.

This tooth tincture, which is quite a favorite, is made in different ways; the compositions made according to the French and English formulas are considered the best. For this and many other tooth tinctures rhatany root is also frequently used. Rhatany root is derived from Krameria triandra, a South American plant. Its alcoholic tincture has a red color.

A. French Formula.

Anise 10 oz.
Cochineal ¾ oz.
Mace 150 grains.
Cloves. 150 grains.
Cinnamon 2¾ oz.
Alcohol 3 qts.
Oil of peppermint ¾ oz.

B. English Formula.

Tincture of cedar 4 qts.
Tincture of myrrh 1 qt.
Tincture of rhatany 1 qt.
Oil of lavender ¾ oz.
Oil of peppermint 1 oz.
Oil of rose 150 grains.

Borated Tooth Tincture.

Borax 5½ oz.
Myrrh 5½ oz.
Red santal wood 5½ oz.
Sugar 5½ oz.
Cologne water 1 qt.
Alcohol 3 qts.
Water 3 pints.

Macerate the myrrh and santal wood in the alcohol, then add the Cologne water, and lastly the sugar and borax dissolved in the water.

Camphorated Cologne Water.

Camphor 1 lb.
Cologne water 4 qts.

Cologne water with myrrh is made in the same way, by substituting a like weight of myrrh for the camphor.

Eau de Milan.

Kino 3½ oz.
Civet 75 grains.
Cinnamon ¾ oz.
Alcohol 5 qts.
Oil of bergamot 150 grains.
Oil of lemon 150 grains.
Oil of peppermint ¾ oz.

Kino contains an astringent, a variety of tannin, and forms a dark red solution with alcohol.

Eau de Mialhe.

Tincture of benzoin ¾ oz.
Tincture of tolu ¾ oz.
Tincture of vanilla 150 grains.
Kino 5½ oz.
Alcohol 5 qts.
Oil of anise. 75 grains.
Oil of peppermint ¾ oz.
Oil of star-anise 75 grains.
Oil of cinnamon 150 grains.

Myrrh Tooth Tincture.

Mace 1¾ oz.
Myrrh. 8 oz.
Cloves 8 oz.
Rhatany root. 8 oz.
Alcohol 5 qts.

Chloral Mouth Wash.

Chloral hydrate 1 oz.
Water 10 oz.

A small quantity of this, rinsed about the mouth, removes every trace of bad odor.

Potassium Permanganate Water.

Potassium permanganate 3½ oz.
Distilled water 5 qts.

Potassium permanganate easily dissolves in distilled water and forms a beautiful violet solution, a few drops of which are placed in a glass of water for use. This salt is one of the most valuable articles for the teeth; it has the property of readily giving off oxygen to organic substances and hence immediately destroys all odor in the mouth by oxidizing the organic bodies; it also removes at once the odor of tobacco smoke. After rinsing the mouth with this solution, it is well to use some peppermint water for polishing the teeth. This mouth wash leaves brown stains on linen and other materials as well as on the skin; such spots can only be removed with acids (hydrochloric, oxalic, etc.).

Salicylated Tooth Tincture.

Salicylic acid 1¾ oz.
Orange-flower water 30 grains.
Water 2 qts.
Alcohol 1 qt.
Oil of peppermint 30 grains.

Salicylic acid is a substance possessing strong antiseptic properties; therefore, when this mouth wash is used after meals, the occurrence of any bad odor, even in persons with defective teeth, is prevented and the progress of caries is arrested, so that the acid may be considered one of the most valuable substances in hygienic perfumery.

Dissolve the salicylic acid in the warm alcohol mixed with water; add to the still warm solution the orange-flower water and the oil of peppermint dissolved in some of the alcohol.

Eau de Salvia.

Oil of lemon. ¾ oz.
Oil of sage 1¾ oz.
Alcohol 1 qt.
Water 4 qts.

The essential oils are dissolved in the alcohol, and this solution mixed with the water.

Eau de Violettes.

Tincture of orris root 1 qt.
Rose water, triple 1 qt.
Alcohol 1 qt.
Oil of bitter almond 75 grains.
Oil of neroli 30 grains.

CHAPTER XXV.
COSMETIC PERFUMERY.

In cosmetic perfumery, use is made chiefly of articles which serve to beautify some parts of the body by artificial means; for instance, to impart to pale cheeks a youthful freshness or to restore to prematurely gray hair its original appearance. In so far as the former object is attained also by the preparations discussed in Chapters XXI., XXII., XXIII., and XXIV., they likewise belong to the domain of cosmetic perfumery; for health and beauty are inseparably connected.

Though we have separated hygienic from cosmetic perfumery, we have done so only in order to draw the line between preparations whose regular use really improves the bodily health, and those which temporarily cover a defect of certain parts of the body.

Cosmetics may also be divided into several groups—those for beautifying the skin, as paints and toilet powders; and those for the care of the hair. The latter are subdivided into hair washes, hair dyes, so-called hair tonics, depilatories, and preparations for dressing the hair, i.e., for making it glossy and fixing it.


CHAPTER XXVI.
SKIN COSMETICS AND FACE LOTIONS.

The use of skin cosmetics and paints is of remote antiquity, but varies in different nations according to their civilization and their sense of beauty. While among certain Oriental nations dark blue rings around the eyes, with yellow lips and nails, pass for beautiful, the European prizes only a white skin with a delicate tinge of red; Italian ladies in the middle ages used the dark red juice of the fruit of the deadly night-shade as a paint, hence the name bella donna, i.e., beautiful lady. (According to Matthiolus, the name herba bella donna arose from the fact that Italian ladies used a distilled water of the plant as a cosmetic.) Owing to its marked effect on the eyes, by dilating the pupil and increasing the lustre, this juice also heightens the brilliancy of the eye, though at the expense of its health.

While in the last century face-painting was a universal fashion, it is nowadays resorted to only by persons whose skin requires some artificial help. But nobody desires that the cosmetic should be perceptible on the skin. Hence it must be laid down as a rule that paints and all cosmetics should be so compounded that it is not easily possible to the observer to recognize that some artificial means has been employed for beautifying the skin.

We give below a number of such articles, which come as near as possible to this ideal without injuring the skin. As every skin cosmetic cannot but occlude the pores of the skin, it should be removed as soon as possible—an advice to be heeded particularly by actors and actresses, who must appear painted on the boards.

A. White Skin Cosmetics.

French White (Blanc Français).